Flow injection sample introduction methods for atomic-absorption spectrometry
نویسندگان
چکیده
منابع مشابه
Determination of lead in wine and rum samples by flow injection-hydride generation-atomic absorption spectrometry.
A method for direct determination of lead in wine and rum samples was developed, using a flow injection hydride generation system coupled to an atomic absorption spectrometer with flame-quartz atomizer (FI-HG-AAS). Lead hyride (PbH(4)) was generated using potassium ferricyanide (K(3)Fe(CN)(6)), as oxidant and sodium tetrahydroborate (NaBH(4)) as reductant. Samples were acidified to 0.40% (v/v) ...
متن کاملDetermination of calcium, magnesium and strontium in soils by flow injection flame atomic absorption spectrometry.
Several procedures for the determination of Ca, Mg and Sr in soils have been compared on the basis of the accuracy of analysis of two NIST reference materials (Montana Soils SRM 2710 and SRM 2711). Samples were dissolved in a mixture of hydrofluoric and nitric acids in sealed vessels in a microwave oven and in teflon beakers on a hot plate. The digests obtained from both dissolution methods wer...
متن کاملApplication of flow injection on-line electrothermal atomic absorption spectrometry to the determination of rhodium.
A fully automated procedure for the determination of rhodium has been developed using flow injection (FI) on-line microcolumn preconcentration coupled with electrothermal atomic absorption spectrometry (ETAAS). The proposed FI manifold and its operation make possible the introduction of the total eluate volume into the graphite atomizer, avoiding the necessity for optimisation of subsampling th...
متن کاملGRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY WITH MAlIlRIX MODIFICATION FOR DETERMINATION OF LEAD IN DRINKING WATER
An amoniumvanadate plus sodium molybdate mixed modifier Graphite Furnace Atomic Absorption Spectrometric method has been developed for determination of traces of lead in drinking water. The concentration of lead in the sample is obtained by direct comparison to linear working graph prepared from aqueous standards in the modifier medium, The results indicate the better performance of the pro...
متن کامل1 Atomic Absorption Spectrometry ( AAS )
Atomic Absorption Spectrometry (AAS) is a technique for measuring quantities of chemical elements present in environmental samples by measuring the absorbed radiation by the chemical element of interest. This is done by reading the spectra produced when the sample is excited by radiation. The atoms absorb ultraviolet or visible light and make transitions to higher energy levels. Atomic absorpti...
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ژورنال
عنوان ژورنال: The Analyst
سال: 1983
ISSN: 0003-2654,1364-5528
DOI: 10.1039/an9830800153